HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 228594Generated: October 31, 2026
Benzophenone, 2'-hydroxy-5'-methoxy- → HCID 24879062, compound
https://huagongshe.com/reaction/228594
Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Benzophenone, 2'-hydroxy-5'-methoxy- | HCID 26881 | — |
| Reactant | 4-Chloro-6,7-dimethoxyquinoline | HCID 459610 | — |
| Product | HCID 24879062 | HCID 24879062 | 8.1% |
Reaction Steps
A mixture of 4-chloro-6,7-dimethoxyquinoline (93 mg) with 2-hydroxy-5-methoxybenzophenone (462 mg) was stirred at 180° C. for 9 hr. The reaction solution was cooled to room temperature and was purified by column chromatography on silica gel using acetone-hexane to give the title compound (14 mg, yield 8%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| Patent number | US07560558B2 |
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| Source dataset | uspto-grants-2009_07 |
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| ORD ID | ord-2e4e47a6537841959febb3d150c4557e |
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| Source note | uspto-grants-2009_07 |
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