Gamma-Butyrolactone → HCID 21847272, compound

HRID 2285944Notes

Reaction equation

HRID 2285944 reaction equation
[CH2:1]([NH2:19])[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH2:12][CH2:13][CH2:14][CH2:15][CH2:16][CH2:17][CH3:18].[C:20]1(=[O:25])[O:24][CH2:23][CH2:22][CH2:21]1>>[OH:25][CH2:20][CH2:21][CH2:22][C:23]([NH:19][CH2:1][CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH2:12][CH2:13][CH2:14][CH2:15][CH2:16][CH2:17][CH3:18])=[O:24]

Participants

3

Reactant 2

HCID 7302Gamma-Butyrolactone2×HCID 15793Octadecylamine

Product 1

HCID 21847272HCID 21847272, compound

Conditions

Temperature
150 °C

Procedure

In a glass reaction vessel, 13.5 grams of octadecylamine were admixed with 4.3 grams of butyrolactone. The mixture was then heated to 150° C. by means of an oil bath until the reaction was complete in a period of 2 hours. A conversion of greater than 95% based on butyrolactone was achieved. Upon cooling to room temperature, the product formed a white to pale yellow, hard, waxy solid. Substantially all of the butyrolactone was reacted indicating greater than 95% conversion.

Workup

  1. temperatureUpon cooling to room temperature
  2. customthe product formed a white to pale yellow, hard, waxy solid

Sources & evidence

ORD record
ord-87e407372d8e415c8ee3f0c2bd3dbb09
Source dataset
uspto-grants-1982_04
Patent number
US04325973

Reaction notes

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