Tert-Butylamine → HCID 20543315, compound

HRID 2286009Notes

Reaction equation

HRID 2286009 reaction equation
[CH2:1]([C:3]1[O:4][CH2:5][CH2:6][N:7]=1)[CH3:2].[C:8]([NH2:12])([CH3:11])([CH3:10])[CH3:9]>C([O-])(=O)C.[Zn+2].C([O-])(=O)C>[C:8]([NH:12][CH2:5][CH2:6][NH:7][C:3](=[O:4])[CH2:1][CH3:2])([CH3:11])([CH3:10])[CH3:9]

Participants

4

Reactant 2

HCID 6385Tert-ButylamineHCID 664122-Ethyl-2-oxazoline

Product 1

HCID 20543315HCID 20543315, compoundYield 64%

Reagents, catalysts & solvents 1

HCID 11192Zinc AcetateCatalyst

Procedure

Under the same conditions as Example 13, 2.5 gm (25 mmoles) of 2-ethyl-2-oxazoline, 1.84 gm (25 mmoles) of t-butylamine and 49.4 mg (0.27 mmole) of zinc acetate are reacted to yield 64 percent N-(2-t-butylaminoethyl)propionamide.

Sources & evidence

ORD record
ord-8b464331d5874b96a35f2ab70a2bc50a
Source dataset
uspto-grants-1982_04
Patent number
US04326067

Reaction notes

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