HuagongsheHuagongshe Chemistry Print Report · For research reference only
Piperidine-1-propylamine → HCID 22819943, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Piperidine-1-propylamine | HCID 19049 | — |
| Reactant | Monomethyl maleate | HCID 5354456 | — |
| Solvent | Triethylamine | HCID 8471 | — |
| Product | HCID 22819943 | HCID 22819943 | — |
Reaction Steps
In a manner analogous to that described in Example 1, 28.6 g (0.2 mol+10% excess) of maleic acid-monomethyl ester, 40 ml of triethylamine and 88.4 g (0.2 mol) of N-(3'-aminopropyl)-piperidine are reacted and the reaction product is purified. The yield is 36.7 g (67.4% of theory) and the melting point of the product obtained is 172°-173° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04326069 |
| Source dataset | uspto-grants-1982_04 |
| ORD ID | ord-58c40167037f40a9b2ad44c3827b91bb |
| Source note | uspto-grants-1982_04 |