HuagongsheHuagongshe Chemistry Print Report · For research reference only
Phenyl isocyanate → HCID 86737666, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Phenyl isocyanate | HCID 7672 | — |
| Reactant | HCID 73683068 | HCID 73683068 | — |
| Catalyst | Triethylamine | HCID 8471 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 86737666 | HCID 86737666 | — |
Reaction Steps
Following the procedure of Example 11, 3 g of 3-(N-chloroacetyl-2,6-dimethylphenylamino)-2-butanone oxime, 3 g phenylisocyanate and 5 drops triethylamine in 100 ml methylene chloride were stirred, refluxed and worked up to yield the title product, m.p. 115°-117° C. This product is tabulated as Compound No. 18 in Table I.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04326077 |
| Source dataset | uspto-grants-1982_04 |
| ORD ID | ord-91137e9e75374b0c973c9c9507204ac4 |
| Source note | uspto-grants-1982_04 |