1-(1H-Imidazol-1-yl)ethanone → HCID 12832895, compound

Participants

Reaction Steps

The mixture of 0.3 g of 4-chloro-3-(2,3-dichlorophenyl)pyrol and 0.6 g of N-acetylimidazole was fused for one hour at 140° C. in a stream of argon. The resulting reaction mixture was purified by thin-layer chromatography to obtain 0.2 g of the desired product (colorless or slightly colored crystal, m.p. 97° C.).

Provenance & Evidence