HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 12831639, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | Ethanol | HCID 702 | — |
| Reactant | HCID 12836706 | HCID 12836706 | — |
| Product | HCID 12831639 | HCID 12831639 | 84.8% |
Reaction Steps
A mixture of 1.49 g 2-allyl-3-oxo-5-methylthio-2,3-dihydro-1,2,4-triazine, 6 ml conc. hydrochloric acid and 12 ml ethyl alcohol was heated under reflux for 1.5 hours. After cooling to room temperature, the solvent was removed under reduced pressure to obtain a yellow solid. This solid was recrystallized from ethyl alcohol to obtain 1.06 g of a white crystal.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04327094 |
| Source dataset | uspto-grants-1982_04 |
| ORD ID | ord-9f8d8784f1314fdb92de2c998aeeb7c8 |
| Source note | uspto-grants-1982_04 |