Hydrochloric Acid → HCID 12836708, compound

Participants

Reaction Steps

A mixture of 1.34 g 2-propargyl-3-methylthio-5-oxo-2,3-dihydro-1,2,4-triazine, 5 ml conc. hydrochloric acid and 10 ml ethyl alcohol was heated under reflux for 1.5 hours. After cooling to room temperature, the solvent was removed under reduced pressure to obtain a yellow solid. This solid was recrystallized from ethyl alcohol to obtain 0.92 g of a white crystal.

Provenance & Evidence