Thiophenol → HCID 15478590, compound

HRID 2286228Notes

Reaction equation

HRID 2286228 reaction equation
[C:1]1([SH:7])[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=1.Cl.[CH3:9][C:10]1[N:15]=[C:14]([CH2:16]Cl)[CH:13]=[CH:12][CH:11]=1.[O-]CC.[Na+]>>[CH3:16][C:14]1[CH:13]=[CH:12][CH:11]=[C:10]([CH2:9][S:7][C:1]2[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=2)[N:15]=1

Participants

4

Reactant 3

HCID 7969ThiophenolHCID 765456-Chloromethyl-2-methylpyridinium chlorideHCID 2723922Sodium ethoxide

Product 1

HCID 15478590HCID 15478590, compound

Procedure

Following the method of Example 1A thiophenol is reacted with 6-methyl-2-picolyl chloride hydrochloride in the presence of sodium ethoxide to give 2-methyl-6-((phenylthio)methyl)pyridine.

Sources & evidence

ORD record
ord-0a6b2bec8e68460b9fb4a6c021294e38
Source dataset
uspto-grants-1982_04
Patent number
US04327102

Reaction notes

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