HCID 15571067, compound → HCID 15571068, compound

Participants

Reaction Steps

The N-(2,2-dimethoxyethyl)-2-[(acetylthio)methyl]-4-methylpentanamide obtained in Example 1 is dissolved in 15 ml of absolute ethanol and the atmosphere is purged with argon. Concentrated ammonium hydroxide (2 ml) is added and this solution is stirred at room temperature for 3 hours, concentrated to dryness in vacuo and dried at 50° C. for 8 hours over phosphorous pentoxide. The title compound (0.8 g) crystallizes, melting point 34°-37° C.

Provenance & Evidence