HCID 15571068, compound → HCID 53860988, compound

HRID 2286247Notes

Reaction equation

HRID 2286247 reaction equation
C[O:2][CH:3](OC)[CH2:4][NH:5][C:6](=[O:14])[CH:7]([CH2:12][SH:13])[CH2:8][CH:9]([CH3:11])[CH3:10]>O.Cl>[SH:13][CH2:12][CH:7]([CH2:8][CH:9]([CH3:11])[CH3:10])[C:6]([NH:5][CH2:4][CH:3]=[O:2])=[O:14]

Participants

4

Reactant 1

HCID 15571068HCID 15571068, compound

Product 1

HCID 53860988HCID 53860988, compound

Reagents, catalysts & solvents 2

HCID 313Hydrochloric AcidCatalystHCID 962WaterSolvent

Procedure

The N-(2,2-dimethoxyethyl)-2-(mercaptomethyl)-4-methylpentanamide obtained in Example 2 is dissolved in 10 ml of water and treated with a few drops of 10% hydrochloric acid. After standing for 1 hour at 25° C., the water is removed in vacuo and the product is obtained as a powder by triturating with acetonitrile.

Workup

  1. customthe water is removed in vacuo
  2. customthe product is obtained as a powder
  3. customby triturating with acetonitrile

Sources & evidence

ORD record
ord-f75c83569f32455eaf2419edc2a2fb11
Source dataset
uspto-grants-1982_04
Patent number
US04327111

Reaction notes

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