HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-tert-Butylbenzoyl chloride → HCID 21464702, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-tert-Butylbenzoyl chloride | HCID 74372 | — |
| Reactant | Methoxydiphenylphosphine | HCID 77636 | — |
| Reactant | 4-Prenylphlorisovalerophenone | HCID 25200610 | — |
| Solvent | Toluene | HCID 1140 | — |
| Product | HCID 21464702 | HCID 21464702 | — |
Reaction Steps
41.3 parts of p-tert.-butylbenzoyl chloride are reacted with 45.4 parts of methoxydiphenylphosphine, dissolved in 20 parts of toluene, in 90 minutes at 50° C., by a method similar to that described for compound X. After evaporating off the solvent on a rotary evaporator, the product is recrystallized from cyclohexane.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04265723 |
| Source dataset | uspto-grants-1981_05 |
| ORD ID | ord-e26c18fde59d48ffada3484bfff8cdd1 |
| Source note | uspto-grants-1981_05 |