HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethenesulfonyl fluoride → N-(2-Fluorosulfonylethyl)-N-ethyl-m-acetamidoaniline
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethenesulfonyl fluoride | HCID 69612 | — |
| Reactant | Acetamide, N-[3-(ethylamino)phenyl]- | HCID 170497 | — |
| Solvent | Isopropanol | HCID 3776 | — |
| Product | N-(2-Fluorosulfonylethyl)-N-ethyl-m-acetamidoaniline | HCID 21161681 | — |
Reaction Steps
N-ethyl-m-acetamidoaniline (178.0 g, 1.0 m is dissolved in isopropyl alcohol (450 ml) and vinylsulfonylfluoride (110 g, 1.0 m) is added dropwise allowing temperature to rise to 40° C. The reaction is stirred for 2.5 hrs., the product collected by filtration, washed with cold ethanol and air dried.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04265812 |
| Source dataset | uspto-grants-1981_05 |
| ORD ID | ord-117db2314f974d80a9808f46e7d24e4b |
| Source note | uspto-grants-1981_05 |