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HRID2286317

反应详情

EQUATION

反应方程式

HRID 2286317 的结构方程式

REACTANTS

反应物

2
结构：C=CS(=O)(=O)F
HCID69612

Ethenesulfonyl fluoride

C2H3FO2S

结构：CCNc1cccc(NC(C)=O)c1
HCID170497

Acetamide, N-[3-(ethylamino)phenyl]-

C10H14N2O

PRODUCTS

生成物

1
结构：CCN(CCS(=O)(=O)F)c1cccc(NC(C)=O)c1
HCID21161681

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

1
结构：CC(C)O
溶剂HCID3776

Isopropanol

C3H8O

PROCEDURE

实验过程

N-ethyl-m-acetamidoaniline (178.0 g, 1.0 m is dissolved in isopropyl alcohol (450 ml) and vinylsulfonylfluoride (110 g, 1.0 m) is added dropwise allowing temperature to rise to 40° C. The reaction is stirred for 2.5 hrs., the product collected by filtration, washed with cold ethanol and air dried.

WORKUP

后处理

  1. customto rise to 40° C
  2. filtration, the product collected by filtration
  3. washwashed with cold ethanol and air
  4. customdried