HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Furanmethanethiol → HCID 23462916, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Furanmethanethiol | HCID 7363 | — |
| Reactant | HCID 12668031 | HCID 12668031 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 23462916 | HCID 23462916 | — |
Reaction Steps
Following the procedures outlined in Example 17, 0.9 g. (0.0075 mole) of furfuryl mercaptan and 2 g. (0.0073 mole) of 3-methyl-2,3,4,5-tetrahydro-1H-3-benzazepine-7,8-dione hydrobromide were reacted in 200 ml. of methanol to yield 7,8-dihydroxy-6-furfurylthio-3-methyl-2,3,4,5-tetrahydro-1H-3-benzazepine, free base m.p. 162°-165° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04265890 |
| Source dataset | uspto-grants-1981_05 |
| ORD ID | ord-4c06edc0efd344a197c42d6c6f141056 |
| Source note | uspto-grants-1981_05 |