HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethyl 3-(m-nitrophenyl)-3-oxopropionate → HCID 23463335, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethyl 3-(m-nitrophenyl)-3-oxopropionate | HCID 104078 | — |
| Reactant | HCID 23463329 | HCID 23463329 | — |
| Solvent | Acetic Acid | HCID 176 | — |
| Solvent | Water | HCID 962 | — |
| Product | HCID 23463335 | HCID 23463335 | — |
Reaction Steps
0.15 Mole (35.6 g) of m-nitrobenzoyl acetic acid ethyl ester and 0.15 mole (25.2 g) of 2,2,2-trifluoroethyl hydrazine hydrate were stirred together for 2 hours in 90 ml of boiling acetic acid. Subsequently, the reaction mixture was poured out in water. After stirring and filtration, the precipitate was recrystallized from methanol.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04266014 |
| Source dataset | uspto-grants-1981_05 |
| ORD ID | ord-fcb5fd1a657f49cda5934042f48a6c2b |
| Source note | uspto-grants-1981_05 |