HuagongsheHuagongshe Chemistry Print Report · For research reference only
Diethyl oxalacetate → HCID 23463328, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Diethyl oxalacetate | HCID 66951 | — |
| Reactant | Sodium | HCID 5360545 | — |
| Reactant | HCID 23463329 | HCID 23463329 | — |
| Solvent | Acetic Acid | HCID 176 | — |
| Product | HCID 23463328 | HCID 23463328 | — |
Reaction Steps
1 Mole (221 g) of the sodium salt of oxalacetic diethyl ester and 1 mole (224 g) of 2,2,2-trifluoroethylhydrazine hydrate were stirred for 1 hour in 1 l of boiling acetic acid. The mixture was poured out on water and stirred. The product melting at 171° C. was filtered with suction.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04266014 |
| Source dataset | uspto-grants-1981_05 |
| ORD ID | ord-3dc6788a4d734aeca8fb7fba33f4a7f8 |
| Source note | uspto-grants-1981_05 |