Ethyl Acetate → HCID 23461629, compound

HRID 2286573Notes

Reaction equation

HRID 2286573 reaction equation
[CH3:1][C:2]1[CH:10]=[CH:9][C:5]([C:6](Cl)=[O:7])=[CH:4][CH:3]=1.[C:11]([CH:13]1[CH2:15][NH:14]1)#[N:12].C(OCC)(=O)C>O>[CH3:1][C:2]1[CH:10]=[CH:9][C:5]([C:6]([N:14]2[CH2:15][CH:13]2[C:11]#[N:12])=[O:7])=[CH:4][CH:3]=1

Participants

5

Reactant 3

HCID 8857Ethyl AcetateHCID 134054-Methylbenzoyl ChlorideHCID 118115Aziridine-2-carbonitrile

Product 1

HCID 23461629HCID 23461629, compound

Reagents, catalysts & solvents 1

HCID 962WaterSolvent

Procedure

This compound is obtained in the form of an oil in a yield of 1.8 g. from 1.54 g. p-methylbenzoyl chloride and 0.68 g. 2-cyanoaziridine. It still contains a little ethyl acetate and water. The analytical results (elementary analysis, NMR and mass spectra) confirm the structure.

Workup

  1. customThis compound is obtained in the form of an oil in a yield of 1.8 g
  2. customThe analytical results (elementary analysis, NMR and mass spectra)

Sources & evidence

ORD record
ord-7584a697ac4e40d39136b1b9d0457e88
Source dataset
uspto-grants-1981_05
Patent number
US04267174

Reaction notes

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