HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 15572235, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | HCID 15572222 | HCID 15572222 | — |
| Solvent | Sodium Hydroxide | HCID 14798 | — |
| Product | HCID 15572235 | HCID 15572235 | — |
Reaction Steps
Dissolve ethyl N-[2,6-dimethyl-4-(hexafluoro-2-hydroxy-2-propyl)phenyl]glycinate (3.1 g, 8.3 mmol) in 25 ml 1.0 N NaOH. After 1 hour, add 25 ml 1.0 N HCl and extract with ethyl acetate. Dry and concentrate. Recrystallize from chloroform-benzene to give the title compound as beige solid, m.p. 153°-155° C. dec.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04267193 |
| Source dataset | uspto-grants-1981_05 |
| ORD ID | ord-cf6f348677f34fa2a6fb539f05d7caf0 |
| Source note | uspto-grants-1981_05 |