HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium Hydroxide → HCID 15572236, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium Hydroxide | HCID 14798 | — |
| Reactant | HCID 15572223 | HCID 15572223 | — |
| Solvent | Hydrochloric Acid | HCID 313 | — |
| Product | HCID 15572236 | HCID 15572236 | — |
Reaction Steps
Stirr ethyl N-[2,6-diisopropyl-4-(hexafluoro-2-hydroxy-2-propyl)phenyl]glycinate (5.0 g, 12 mmol) with 50 ml 1.0 N NaOH for 1 hour. Neutralize the solution with 50 ml 1.0 N HCl. Filter the solid, dissolve in ether, dry and concentrate. Recrystallize from ether-hexane to obtain the title compound as a white solid, m.p. 130°-132° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04267193 |
| Source dataset | uspto-grants-1981_05 |
| ORD ID | ord-876fef8aafc14a45a095b54eb42916f7 |
| Source note | uspto-grants-1981_05 |