Hydrochloric Acid → HCID 86754565, compound

Participants

Reaction Conditions

Reaction Steps

L-Cysteine (157.4 g) was added to 250 ml of decyl alcohol saturated with dry HCl. The mixture was heated to 150° C. for 6 hours. The solution was cooled and was mixed with an equal volume of ethyl acetate. The solution was cooled in a dry ice bath to give crystals. The crystals were filtered and were then recrystallized from ethyl acetate, mp 96°-99° C., yield 100 g, IR (KBr) 1745 cm-1.

Provenance & Evidence