HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethyl Bromide → HCID 23460465, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethyl Bromide | HCID 6332 | — |
| Reactant | Triethyl phosphite | HCID 31215 | — |
| Reactant | HCID 22913727 | HCID 22913727 | — |
| Solvent | Water | HCID 962 | — |
| Product | HCID 23460465 | HCID 23460465 | 78% |
Reaction Steps
A mixture of 12.38 g of 4(p-chlorophenyl)butyl bromide and 20 g of triethyl phosphite was refluxed at 160° for seven hours. During this period the circulating water in the condenser was maintained at 50° to allow the ethyl bromide to distill off. After removal of the excess of triethyl phosphite, distillation under reduced pressure gave 11.9 g (39 mmol) of a white viscuous oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04268507 |
| Source dataset | uspto-grants-1981_05 |
| ORD ID | ord-6e5c8cc9bc3d44d69faa815653f49241 |
| Source note | uspto-grants-1981_05 |