Hexane → HCID 54522606, compound

Participants

Reaction Steps

A solution of 33 g of 4-chloro-3-nitro-benzoyl chloride in 100 ml of benzene is added dropwise in the course of one hour to a solution, which has been heated to the reflux temperature, of 54.3 g of N-n-hexadecyl-2-nitroaniline in 80 ml of benzene. After a further two hours, the reaction has ended. The reaction solution is poured into 600 ml of hexane and the mixture is left to stand overnight. The resulting crystals are filtered off with suction and washed with hexane. This gives 48 g of the compound with a melting point of 83° to 85° C.

Provenance & Evidence