HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloride methanol → HCID 68828808, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloride methanol | HCID 21893726 | — |
| Reactant | HCID 24879270 | HCID 24879270 | — |
| Product | HCID 68828808 | HCID 68828808 | 10% |
Reaction Steps
1-[2-(6,7-Dimethoxy-quinolin-4-yloxy)-5-methoxy-phenyl]-ethanone (802 mg) was dissolved in a hydrochloric acid-methanol solution (20 ml) to prepare a solution which was then stirred at room temperature overnight. The solvent was removed by distillation under the reduced pressure, and the residue was washed with ethyl acetate and was dried in vacuo to give the title compound (885 mg, yield 10%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07560558B2 |
| Source dataset | uspto-grants-2009_07 |
| ORD ID | ord-dd4b7784496c484597ddfe3f571fcfa8 |
| Source note | uspto-grants-2009_07 |