Back
HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 2287029Generated: November 1, 2026

Hydroxyamine hydrochloride → HCID 13078361, compound

https://huagongshe.com/reaction/2287029

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHydroxyamine hydrochlorideHCID 443297—
ReactantHCID 514045HCID 514045—
SolventPyridineHCID 1049—
ProductHCID 13078361HCID 13078361—

Reaction Steps

4-[6-(4-Bromophenoxy)hexyl]-3,5-diethylisoxazole [I; Ar is 4-BrC6H4, Y is O(CH2)6, R is C2H5 ] was prepared from 10.0 g. of 4-[6-(4-bromophenoxy)hexyl]-3,5-heptanedione and 2.0 g. of hydroxylamine hydrochloride in 40 ml. of pyridine according to the procedure of Example 2, part (b), and was obtained in the form of a pale yellow oil, b.p. 190°-195° C. (0.001 mm.); yield 7.3 g.; MIC=12 μg/ml (herpes 2).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS04268678
Source datasetuspto-grants-1981_05
ORD IDord-3c5afdaaf739491ea0ac64cc31f689c8
Source noteuspto-grants-1981_05