HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydroxyamine hydrochloride → HCID 13078361, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydroxyamine hydrochloride | HCID 443297 | — |
| Reactant | HCID 514045 | HCID 514045 | — |
| Solvent | Pyridine | HCID 1049 | — |
| Product | HCID 13078361 | HCID 13078361 | — |
Reaction Steps
4-[6-(4-Bromophenoxy)hexyl]-3,5-diethylisoxazole [I; Ar is 4-BrC6H4, Y is O(CH2)6, R is C2H5 ] was prepared from 10.0 g. of 4-[6-(4-bromophenoxy)hexyl]-3,5-heptanedione and 2.0 g. of hydroxylamine hydrochloride in 40 ml. of pyridine according to the procedure of Example 2, part (b), and was obtained in the form of a pale yellow oil, b.p. 190°-195° C. (0.001 mm.); yield 7.3 g.; MIC=12 μg/ml (herpes 2).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04268678 |
| Source dataset | uspto-grants-1981_05 |
| ORD ID | ord-3c5afdaaf739491ea0ac64cc31f689c8 |
| Source note | uspto-grants-1981_05 |