2-Methoxy-4-nitroaniline → HCID 20565335, compound

HRID 2287110Notes

Reaction equation

HRID 2287110 reaction equation
[NH2:1][C:2]1[CH:19]=[CH:18][C:5]([C:6](NC2C=CC(N)=CC=2OC)=[O:7])=[CH:4][CH:3]=1.COC1C=C([N+]([O-])=O)C=CC=1N.[Cl:32][C:33]1[CH:39]=[C:38]([N+:40]([O-])=O)[CH:37]=[C:36]([Cl:43])[C:34]=1[NH2:35]>>[NH2:1][C:2]1[CH:19]=[CH:18][C:5]([C:6]([NH:35][C:34]2[C:33]([Cl:32])=[CH:39][C:38]([NH2:40])=[CH:37][C:36]=2[Cl:43])=[O:7])=[CH:4][CH:3]=1

Participants

4

Reactant 3

HCID 73372-Methoxy-4-nitroanilineHCID 74302,6-Dichloro-4-nitroanilineHCID 138398764-Amino-N-(4-amino-2-methoxyphenyl)benzamide

Product 1

HCID 20565335HCID 20565335, compound

Procedure

By operating as described under (a) above, but using instead of 202 parts of 2-methoxy-4-nitro-aniline, 248 parts of 2,6-dichloro-4-nitro-aniline, high yields of 4,4'-diamino-2'6'-dichloro-benzanilide were obtained.

Sources & evidence

ORD record
ord-35d28761a76b4704ad62ee81aae07672
Source dataset
uspto-grants-1981_05
Patent number
US04269769

Reaction notes

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