Hydrochloric Acid → HCID 23459451, compound

Participants

Reaction Steps

Methanesulfonic acid 2-(1-phenyl-2,5-cyclohexadien-1-yl)-ethyl ester is reacted with methylamine by an analogous procedure to that described in Example 7. The crude product obtained is converted in the usual manner into the hydrochloride which is recrystallized from isopropanol. There is obtained N-methyl-1-phenyl-2,5-cyclohexadien-1-ethylamine hydrochloride having a melting point of 172°-173° C.

Provenance & Evidence