HuagongsheHuagongshe Chemistry Print Report · For research reference only
Cyanuric chloride → 2-Chloro-4,6-di(2,3,3-trimethyl-2-butyl)amino-s-triazine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Cyanuric chloride | HCID 7954 | — |
| Reactant | Sodium Hydroxide | HCID 14798 | — |
| Reactant | (1,1,2,2-Tetramethylpropyl)amine hydrochloride | HCID 12321758 | — |
| Solvent | Water | HCID 962 | — |
| Product | 2-Chloro-4,6-di(2,3,3-trimethyl-2-butyl)amino-s-triazine | HCID 15572577 | — |
Reaction Steps
6.7 g. (0.044 mole) 2,3,3-trimethyl-2-butylamine hydrochloride and 3.4 g. (0.84 mole) NaOH in 20 ml. water are added to a stirred slurry of 3.6 g. (0.02 mole) cyanuric chloride in 150 ml. water. The reaction mixture is heated at reflux for 21/2 hours, cooled and filtered to give the product, a white solid, m.p. 129°-131° C., 6.5 g.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04269832 |
| Source dataset | uspto-grants-1981_05 |
| ORD ID | ord-33b4002ee02146238e9f32a7d49dc2c0 |
| Source note | uspto-grants-1981_05 |