HuagongsheHuagongshe Chemistry Print Report · For research reference only
Pyridine-2-carbonitrile → HCID 23459576, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Pyridine-2-carbonitrile | HCID 7522 | — |
| Reactant | 2-Methylbenzonitrile | HCID 10721 | — |
| Reactant | 6-Methylpyridine-2-carbonitrile | HCID 74182 | — |
| Reactant | 4-Chloro-2-methylbenzonitrile | HCID 142742 | — |
| Product | HCID 23459576 | HCID 23459576 | — |
Reaction Steps
Using the method of Example VII, but substituting 2-cyano-6-methylpyridine for the 2-cyanopyridine and 2-methylbenzonitrile for the 4-chloro-2-methylbenzonitrile, there was obtained 1-amino-3-(6-methyl-2-pyridyl)-isoquinoline hydrochloride. The compound was crystallized from isopropyl alcohol. Melting point 263.5°-264.5° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04269834 |
| Source dataset | uspto-grants-1981_05 |
| ORD ID | ord-eea90acce54c45feb8947291183e3099 |
| Source note | uspto-grants-1981_05 |