HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzoyl chloride → HCID 13384145, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzoyl chloride | HCID 7412 | — |
| Reactant | Triethylamine | HCID 8471 | — |
| Reactant | HCID 13384132 | HCID 13384132 | — |
| Solvent | Chloroform | HCID 6212 | — |
| Product | HCID 13384145 | HCID 13384145 | — |
Reaction Steps
The amine prepared as described in (a) was dissolved in chloroform and equivalent amounts of benzoyl chloride and triethylamine were added. The reaction mixture was refluxed for two hours and then washed with water and dried with sodium sulphate. The solvent was distilled off and the residue crystallised from ethanol to yield N-[2-phenyl-1-(2-pyridyl)ethyl]benzamide.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04269834 |
| Source dataset | uspto-grants-1981_05 |
| ORD ID | ord-ab96334872224ff590e618037372af1b |
| Source note | uspto-grants-1981_05 |