HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 23459882, compound → HCID 23459883, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 23459882 | HCID 23459882 | — |
| Reactant | Phthalimide potassium salt | HCID 24194345 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | HCID 23459883 | HCID 23459883 | — |
Reaction Steps
A mixture of 16.3 g of 2'-chloro-5'-tetradecyloxycarbonylchloro-benzoylacetanilide and 18.5 g of phthalimide potassium was stirred in 300 ml of dimethylformamide for 3 hours at room temperature. The reaction product thus obtained was treated as in Synthesis example 1. Upon recrystallizing the product from methanol, 12 g of Coupler 6 having a melting point of 81°-82° C. was obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04269936 |
| Source dataset | uspto-grants-1981_05 |
| ORD ID | ord-7bb93c66faab4593ba41579af29e0371 |
| Source note | uspto-grants-1981_05 |