HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methanol, 1,1-diethoxy-, 1-acetate → HCID 13017518, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methanol, 1,1-diethoxy-, 1-acetate | HCID 84166 | — |
| Reactant | HCID 13017517 | HCID 13017517 | — |
| Solvent | Hexane | HCID 8058 | — |
| Product | HCID 13017518 | HCID 13017518 | — |
Reaction Steps
A mixture of 2.0 g. of 5-(4-chlorophenyl)-4-hydrazinopyrimidine is shaken with 10 ml. of diethoxymethyl acetate. The mixture is allowed to stand 15-30 minutes and then is diluted with hexane. The precipitated product (1.81 g: 83%) is collected and recrystallized from ethanol to give the title compound; m.p. 193°-195° C .
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04269980 |
| Source dataset | uspto-grants-1981_05 |
| ORD ID | ord-93a9b87f16174698ac2065b3be6c13a3 |
| Source note | uspto-grants-1981_05 |