HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 13017518, compound → HCID 13017519, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 13017518 | HCID 13017518 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 13017519 | HCID 13017519 | — |
Reaction Steps
A mixture of 1.76 g. of 8-(4-chlorophenyl)-1,2,4-triazolo[4,3-c]pyrimidine and 25 ml. of methanol is heated at the reflux temperature for 18 hours. The reaction mixture is cooled to room temperature to separate a crystalline material which is collected by filtration to give 1.53 g. (83%) of the product of the example, m.p. 154°-155° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04269980 |
| Source dataset | uspto-grants-1981_05 |
| ORD ID | ord-b7a73640808f40fdacaf73a442dde3aa |
| Source note | uspto-grants-1981_05 |