HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethane, 2-bromo-1,1-diethoxy- → HCID 15888248, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethane, 2-bromo-1,1-diethoxy- | HCID 74852 | — |
| Reactant | HCID 178449019 | HCID 178449019 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 15888248 | HCID 15888248 | — |
Reaction Steps
A solution of the compound of Example 248 and a slight excess of bromoacetaldehyde diethyl acetal in ethanol is heated to reflux until the starting material is consumed. The reaction mixture is evaporated, and the residual material is purified by chromatography or recrystallization to afford the title product.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06083948 |
| Source dataset | uspto-grants-2000_07 |
| ORD ID | ord-b4c674b4816f4a8fbcd90c27afdcb813 |
| Source note | uspto-grants-2000_07 |