Trifluoroacetic acid → HCID 18704612, compound

Participants

Reaction Steps

To a solution of N,N',N'-trimethylhydrazinecarboxylic acid tert-butyl ester (0.52 g, 2.99 mmol) in methylene chloride (4 ml) was added trifluoroacetic acid (4 ml) and the mixture was stirred for 60 min. The mixture was concentrated in vacuo and stripped three times with methylene chloride to give 0.61 g of N,N,N'-trimethylhydrazine trifluoroacetate as a thin oil.

Provenance & Evidence