Trifluoroacetic acid → HCID 18704612, compound

HRID 2287903Notes

Reaction equation

HRID 2287903 reaction equation
C(O[C:6]([N:8]([CH3:12])[N:9](C)[CH3:10])=O)(C)(C)C.[F:13][C:14]([F:19])([F:18])[C:15]([OH:17])=[O:16]>C(Cl)Cl>[F:13][C:14]([F:19])([F:18])[C:15]([OH:17])=[O:16].[CH3:6][N:8]([CH3:12])[NH:9][CH3:10]

Participants

4

Reactant 2

HCID 6422Trifluoroacetic acidHCID 10559152N,N',N'-trimethylhydrazinecarboxylic acid tert-butyl ester

Product 1

HCID 18704612HCID 18704612, compound

Reagents, catalysts & solvents 1

HCID 6344DichloromethaneSolvent

Procedure

To a solution of N,N',N'-trimethylhydrazinecarboxylic acid tert-butyl ester (0.52 g, 2.99 mmol) in methylene chloride (4 ml) was added trifluoroacetic acid (4 ml) and the mixture was stirred for 60 min. The mixture was concentrated in vacuo and stripped three times with methylene chloride to give 0.61 g of N,N,N'-trimethylhydrazine trifluoroacetate as a thin oil.

Workup

  1. concentrationThe mixture was concentrated in vacuo

Sources & evidence

ORD record
ord-f63718149d1b4811bb8495c27d317057
Source dataset
uspto-grants-2000_07
Patent number
US06083908

Reaction notes

Loading…