Methyl formate → HCID 18704597, compound

Participants

Reaction Steps

A solution of N-aminopiperidine (2.0 ml, 18.5 mmol) and methylformate (2.3 ml, 37 mmol) was stirred for four days in a sealed tube at 40° C. The mixture was concentrated in vacuo, suspended in ether (100 ml) and filtered to give 1.84 g of N-(piperidin-1-yl)formamide as a white powder.

Provenance & Evidence