Methyl iodide → HCID 86755501, compound

Participants

Reaction Steps

To a stirred solution of 2 g of 6-methyl-8β-methyl-[5-(5-bromo-pyridin-3-yl)-1,2,4-oxadiazol-3-yl]-10α-methoxy-ergoline in ml 30 of dimethylsulphoxide was added at room temperature, 0.5 g of finely ground sodium hydroxyde. After stirring for 30 mins., a solution of 0.9 g of methyl iodide in m 10 of dimethylsulphoxide was added and the stirring was continued for 1 hour.

Provenance & Evidence