HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sulfuryl chloride → HCID 86755503, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sulfuryl chloride | HCID 24648 | — |
| Reactant | HCID 86755504 | HCID 86755504 | — |
| Solvent | Acetonitrile | HCID 6342 | — |
| Product | HCID 86755503 | HCID 86755503 | — |
Reaction Steps
To a stirred solution of 2 g of 1,6-dimethyl-8β-methyl[3-(5-bromo-pyridin-3-yl)-1,2,4-oxadiazol-5-yl]-10α-methoxy-ergoline in ml 50 of acetonitrile and ml 0.5 of BF3-2 Et2O was added dropwise a solution of 0.6 g of sulphuryichloride (SO2Cl2) in ml 15 of acetonitrile at -5° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06087371 |
| Source dataset | uspto-grants-2000_07 |
| ORD ID | ord-4dd7f97a94244bc7a8a4b77d2db38c01 |
| Source note | uspto-grants-2000_07 |