HuagongsheHuagongshe Chemistry Print Report · For research reference only
Thionyl Chloride → HCID 22342920, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Thionyl Chloride | HCID 24386 | — |
| Reactant | 4-Morpholinobut-2-YN-1-OL | HCID 3112849 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 22342920 | HCID 22342920 | — |
Reaction Steps
Thionyl chloride (2.1 ml) was added to a solution of 4-morpholino-2-butyn-1-ol (1.47 g) in dichloromethane (10 ml) with ice bath cooling. After stirring for 0.5 hour, the solution was evaporate din vacuo. The residue was triturated with ethyl acetate to give 4-morpholino-2-butynyl chloride hydrochloride (1.91 g).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06087357 |
| Source dataset | uspto-grants-2000_07 |
| ORD ID | ord-934a48dd08f942d89baafcaaa59998c3 |
| Source note | uspto-grants-2000_07 |