HRID2288374

反应详情

EQUATION

反应方程式

REACTANTS

反应物

HCID313

Hydrochloric Acid

ClH

HCID517111

Ammonium carbonate

CH8N2O3

结构：Cn1c(COc2cccc(C#N)c2)nc2cc(S(=O)(=O)N3CCCC3)ccc21

HCID18412506

未命名化合物

PRODUCTS

生成物

结构：Cl.Cn1c(COc2cccc(C(=N)N)c2)nc2cc(S(=O)(=O)N3CCCC3)ccc21

HCID18412414

未命名化合物

收率 71%

AUXILIARIES

试剂、催化剂与溶剂

溶剂HCID702

Ethanol

C2H6O

PROCEDURE

实验过程

Prepared analogously to Example 32 from 1-methyl-2-[(3-cyanophenyl)oxymethyl]-benzimidazol-5-yl-sulphonic acid-pyrrolidide, ethanolic hydrochloric acid, ethanol and ammonium carbonate. Yield: 71% of theory, C20H23N5O3S (413.5) EKA mass spectrum: (M+H)+ =414