HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium Hydroxide → HCID 18412732, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium Hydroxide | HCID 14798 | — |
| Reactant | HCID 18412612 | HCID 18412612 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 18412732 | HCID 18412732 | 57% |
Reaction Steps
Prepared analogously to Example 10 from 1-methyl-2-[(4-amidinophenyl)methylthio]-benzimidazol-5-yl-carboxylic acid-N-phenyl-N-(2-ethoxycarbonylethyl)-amide-hydrochloride and sodium hydroxide solution. Yield: 57% of theory, C26H25N5O3S (487.58) Rf value: 0.23 (Reversed Phase silica gel RP-8; Methanol/5% saline solution=6:4) ##EQU93##
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06087380 |
| Source dataset | uspto-grants-2000_07 |
| ORD ID | ord-6795a61fe3764532a09a815a52d2dee2 |
| Source note | uspto-grants-2000_07 |