HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 18412630, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | Ammonium Carbonate | HCID 517111 | — |
| Reactant | HCID 18412586 | HCID 18412586 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 18412630 | HCID 18412630 | 33% |
Reaction Steps
Prepared analogously to Example 25d from 1-methyl-2-[N-(4-cyanophenyl)-aminomethyl]-5-(isoindolin-2-yl-sulphonyl)-benzimidazole and ethanolic hydrochloric acid, ethanol and ammonium carbonate. Yield: 33% of theory, Rf value: 0.32 (silica gel; dichloromethane/methanol=4:1) C24H24N6O2S (460.6) EKA mass spectrum: (M+H)+ =461
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06087380 |
| Source dataset | uspto-grants-2000_07 |
| ORD ID | ord-50ea38eb06cb4f1e9ca34285422a129d |
| Source note | uspto-grants-2000_07 |