HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium Hydroxide → HCID 18412628, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium Hydroxide | HCID 14798 | — |
| Reactant | HCID 18412564 | HCID 18412564 | — |
| Reactant | Ethyl acetate ethanol ammonia | HCID 86587043 | — |
| Product | HCID 18412628 | HCID 18412628 | 92% |
Reaction Steps
Prepared analogously to Example 2 from 3-methyl-2-[2-(4-amidinophenyl)ethyl]-imidazo[1.2-a]pyridin-7-yl-carboxylic acid-N-phenyl-N-(2-ethoxycarbonylethyl)-amide-hydrochloride and sodium hydroxide solution. Yield: 92% of theory, C27H27N5O3 (469.55) Rf value: 0.19 (silica gel; ethyl acetate/ethanol/ammonia=50:45:5) ##EQU119##
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06087380 |
| Source dataset | uspto-grants-2000_07 |
| ORD ID | ord-dc41be6a7124433da7801fedadb4ee1f |
| Source note | uspto-grants-2000_07 |