HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium Hydroxide → HCID 140409620, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium Hydroxide | HCID 14798 | — |
| Reactant | HCID 140409598 | HCID 140409598 | — |
| Solvent | Dichloromethane methanol | HCID 21226129 | — |
| Product | HCID 140409620 | HCID 140409620 | 62% |
Reaction Steps
Prepared analogously to Example 104 from 1-methyl-2-[N-[4-(N-benzyloxycarbonylamidino)phenyl]-aminomethyl]-benzimidazol-5-yl-carboxylic acid-N-(2-pyridyl)-N-(2-ethoxycarbonylethyl)-amide and sodium hydroxide solution. Yield: 62% of theory, C33H31N7O5 (605.7) Rf value: 0.26 (silica gel; dichloromethane/methanol=9:1) ##EQU133##
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06087380 |
| Source dataset | uspto-grants-2000_07 |
| ORD ID | ord-d519fafc6fc6412c85a37dac4ad9b3a2 |
| Source note | uspto-grants-2000_07 |