Acetone → HCID 54041279, compound

Participants

Reaction Steps

Into a four-necked flask equipped with an agitator, a reflux condenser, a thermometer and a dropping apparatus were charged 135 g of (4-amino)acetophenone, 101 g of triethylamine, 500 ml of acetone and 0.5 g of methoxyphenol. To the reaction mixture was then added dropwise 105 g of methacryloyl chloride at a temperature of 10° C. in 2 hours. To the reaction solution was then added 1 l of distilled water. The resulting crystal was recovered by filtration. (Yield: 78%)

Provenance & Evidence