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HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
HRID 2288572Erstellt: 25. Oktober 2026

Methyl triflate → HCID 15476282, Verbindung

https://huagongshe.com/reaction/2288572

Reaktionsgleichung

Beteiligte Stoffe

RolleNameHCIDEinwaage
EduktMethyl triflateHCID 9526—
EduktPhenyl acridine-9-carboxylateHCID 517916—
LösungsmittelDichloromethaneHCID 6344—
ProduktHCID 15476282HCID 15476282—

Reaktionsschritte

Phenyl acridine-9-carboxylate (530 mg, 1.7 mmol) was dissolved in CH2Cl2 (5 mL) under argon and methyl triflate (1 mL, 8.8 mmol) was added. The solution was stirred overnight at room temperature to yield a thick yellow precipitate. This precipitate was filtered, washed with ether and dried to obtain the product as yellow crystals. 1H NMR (acetone-d6) δ 5.22 (s, 3H), 7.47-7.71 (m, 5H), 8.23-9.07 (m, 8H).

Herkunft & Nachweise

DOI10.6084/m9.figshare.5104873.v1
PatentnummerUS06090571
Quelldatensatzuspto-grants-2000_07
ORD IDord-ccd31068837e4f0483912c6297c5bf4a
Quellennotizuspto-grants-2000_07