HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Methyl triflate → HCID 15476282, Verbindung
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Methyl triflate | HCID 9526 | — |
| Edukt | Phenyl acridine-9-carboxylate | HCID 517916 | — |
| Lösungsmittel | Dichloromethane | HCID 6344 | — |
| Produkt | HCID 15476282 | HCID 15476282 | — |
Reaktionsschritte
Phenyl acridine-9-carboxylate (530 mg, 1.7 mmol) was dissolved in CH2Cl2 (5 mL) under argon and methyl triflate (1 mL, 8.8 mmol) was added. The solution was stirred overnight at room temperature to yield a thick yellow precipitate. This precipitate was filtered, washed with ether and dried to obtain the product as yellow crystals. 1H NMR (acetone-d6) δ 5.22 (s, 3H), 7.47-7.71 (m, 5H), 8.23-9.07 (m, 8H).
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US06090571 |
| Quelldatensatz | uspto-grants-2000_07 |
| ORD ID | ord-ccd31068837e4f0483912c6297c5bf4a |
| Quellennotiz | uspto-grants-2000_07 |