HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 54171432, compound → HCID 18699630, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 54171432 | HCID 54171432 | — |
| Solvent | Toluene | HCID 1140 | — |
| Product | HCID 18699630 | HCID 18699630 | — |
Reaction Steps
1-Methylpiperidine-4-carboxylic acid (2-thiophen-3-yl-ethyl)-amide (1.2 g) POCl3 (1.22 ml) were reacted in toluene (50 ml) exactly as described in example 4. 1.1 g of [7-(1-Methylpiperidin-4-yl)-4,5,-dihydrothieno[2,3-c]pyridine was isolated identified by NMR and MS: M+=234.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06090797 |
| Source dataset | uspto-grants-2000_07 |
| ORD ID | ord-a5c4a8f5a70a413ca0b2ff95b28ac6d6 |
| Source note | uspto-grants-2000_07 |