HuagongsheHuagongshe Chemistry Print Report · For research reference only
p-Anisoyl chloride → HCID 9929318, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | p-Anisoyl chloride | HCID 7477 | — |
| Reactant | Triethylamine | HCID 8471 | — |
| Reactant | HCID 18699630 | HCID 18699630 | — |
| Solvent | Toluene | HCID 1140 | — |
| Product | HCID 9929318 | HCID 9929318 | 90% |
Reaction Steps
7-(1-Methylpiperidin-4-yl)-4,5,-dihydrothieno[2,3-c]pyridine (0.1 g), 4-methoxybenzoyl chloride (0.086 g), and triethylamine (0.112 ml ) were reacted in toluene (5 ml) exactly as described in example 4. Yield 90% of crude [7-(1-Methylpiperidin-4-yl)-4,5,6,7-tetrahydrothieno[2,3-c]pyridin-6-yl]-(4-methoxyphenyl)-methanone. MS: M+=370.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06090797 |
| Source dataset | uspto-grants-2000_07 |
| ORD ID | ord-a32e187f9c6942848aa040bcbe380752 |
| Source note | uspto-grants-2000_07 |