HuagongsheHuagongshe Chemistry Print Report · For research reference only
Toluene → HCID 18699636, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Toluene | HCID 1140 | — |
| Reactant | Phosphorus oxychloride | HCID 24813 | — |
| Reactant | HCID 53707289 | HCID 53707289 | — |
| Product | HCID 18699636 | HCID 18699636 | — |
Reaction Steps
Tetrahydro-3-furoic acid (2-thiophen-3-yl-ethyl)-amide(3.35 g), POCl3 (4.06 ml) were reacted in toluene (150 ml) exactly as described in example 4. 2.77 g of 4-tetrahydrofuran-3-yl-4,5,-dihydrothieno[2,3-c]pyridine was isolated identified by NMR and MS: M+=207.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06090797 |
| Source dataset | uspto-grants-2000_07 |
| ORD ID | ord-a4fd1d8956814a34bd6fa9bdbae240d2 |
| Source note | uspto-grants-2000_07 |